A Crystal Camera for Ultra-Small-Angle X-Ray Scattering Using Synchrotron Radiation

Article type: Research Article

Authors: Pahl, R. | Bonse, U.

Affiliations: lnstitut für Physik, Universität Dortmund, Postfach, D-44221 Dortmund, Germany

Abstract: We describe a novel USAXS camera that combines the use of synchrotron radiation with collimation by perfect-crystal optics. The outstanding result is that high measuring intensities and extreme angular resolution are achieved even with a point-focusing geometry. Along the principles of the original design (U. Bonse and M. Hart, Z. Phys. 189, 151 (1966)) which had to be operated at an x-ray tube, we employ two sets of pairs of multiply reflecting channel-cut crystals diffracting in the horizontal and vertical planes. The collimation characteristics thus obtained are equivalent to the point-focusing geometry of conventional SAXS cameras based on slit collimation. We present results from samples of polystyrene spheres which were used for test measurements performed with synchrotron radiation of DORIS at HASYLAB/DESY in Hamburg. Taking into account the number of reflections within the channel-cut crystals, the theoretical resolution was calculated and found to agree well with that derived from measured scattering patterns. Structures as large as about 1.3 μm could easily be identified from the scattering curves. As expected with point-focusing geometry, desmearing of raw data was unnecessary.

DOI: 10.3233/XST-1995-5402

Journal: Journal of X-Ray Science and Technology, vol. 5, no. 4, pp. 368-378, 1995