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Article type: Research Article
Authors: Bourbia, A. | Draissia, M. | Bedboudi, H. | Boulkhessaim, S. | Debili, M.Y.
Affiliations: Laboratory of Magnetism and Spectroscopy of Solids, Physics Department, Faculty of Science, Badji-Mokhtar University, Annaba, Algeria
Note: [] Corresponding author: M. Draissia, Laboratory of Magnetism and Spectroscopy of Solids, Physics Department, Faculty of Science, Badji-Mokhtar University, PB 12 Annaba 23000, Algeria Tel./Fax: +213 38 87 53 96; E-mail: [email protected]
Abstract: This article deals with the microstructural strengthening mechanisms of aluminium by means of hard α-Al_{2}O_{3} alumina fine particles. A broad of understanding views covering materials preparations, elaboration process, characterization techniques and associated microstructural characteristic parameters measurements is given. In order to investigate the microstructural characteristic parameters and the mechanical strengthening mechanisms of pure aluminium by hard fine particles, a set of Al-(α-Al_{2}O_{3}) alloys samples were made under vacuum by high fusion temperature melting, the high frequency (HF) process, and rapidly solidified under ambient temperature from a mixture of cold-compacted high-pure fine Al and α-Al_{2}O_{3} powders. The as-solidified Al-(α-Al_<FORMULA>_{2}O_{3}) alloys were characterized by means of X-ray diffraction (XRD) analyses, optical microscopy observations and Vickers microhardness tests in both brut and heat-treated states. It was found that the as-solidified HF Al-(α-Al_{2}O_{3}) alloys with compositions below 4 wt.% (α-Al_{2}<FORMULA>_O<FORMULA>_{3}) are single-phase microstructures of the solid solution FCC Al phase and over two-phase microstructures of the solid solution FCC Al and the Rhombohedral α-Al_{2}O_{3} phases. The optical micrographs reveal the presence of a grain size refinement in these alloys. Vickers microhardness of the as-solidified Al-(α-Al_{2}O_{3}) is increased by means of pure fine α-Al_{2}O_{3} alumina particles. These combined effects of strengthening and grain size refinement observed in the as-solidified Al-(α-Al_{2}O_{3}) alloys are essentially due to a strengthening of Al by the α-Al_{2}O_{3} alumina particles insertion in the (HF) melted and rapidly solidified alloys.
Keywords: HF fusion, Aluminium alloys, α-Al[TeX:] _{2}O[TeX:] _{3} alumina fine particles, Microstructure characteristic parameters, Strengthening mechanisms
DOI: 10.3233/XST-2010-0245
Journal: Journal of X-Ray Science and Technology, vol. 18, no. 2, pp. 201-219, 2010
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