Abstract: TiO_2 nanotube precursor was synthesized by the
hydrothermal reaction of TiO_2 powders with NaOH solution
and the properties of the nanotube materials were tuned using different
post-treatments. Transmission electron microscopic (TEM) observation revealed
that the nanotube could be obtained by either a direct rinse with acid solution
or rinse with distilled water followed by acid solution. The results of X-ray
diffraction (XRD) and inductively coupled plasma (ICP) analysis indicated that
the nanotube material was composed of
H_2Ti_2O_5·H_2.
In addition, the photocaalytic activities of the resulting catalysts were found
to be strongly dependent on the post-treatment. The results of the
photocatalytic reaction showed that the degradation of Acid-red 3B dye fitted
pseudo-zero-order kinetics and TiO_2 nanotube prepared under
direct rinse with acid solution exhibited a higher catalytic efficiency
compared to other catalysts.